A simple cladding procedure was developed to apply monolithic silica rods in chromatography. This was used to evaluate the performances of new monolithic silica phases synthesised using a triblock copolymer as a phase separation inducer. The cladding procedure is found efficient after several tests, including scanning electron microscopy and mercury porosimetry, and the obtained columns present a relatively good efficiency in adsorption chromatography (H min is about 50 μm) as compared to other lab-scale developed columns.
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