Simultaneous determination of pyrethrins residues in teas by ultra-performance liquid chromatography/tandem mass spectrometry

Anal Chim Acta. 2010 Sep 23;678(1):56-62. doi: 10.1016/j.aca.2010.08.015. Epub 2010 Aug 20.

Abstract

A sensitive and effective method for the simultaneous quantitative determination of pyrethrin residues in teas was developed and validated using ultra-performance liquid chromatography coupled with tandem mass spectrometry (UPLC-MS/MS). The six major constituents of the pyrethrins (pyrethrin I and II, jasmolin I and II, and cinerin I and II) were successfully separated and independently confirmed in a single run within approximately 5 min. The multi-residue analysis of pyrethrins in teas involved simply extraction with acetonitrile, clean-up using a multilayer solid phase extraction cartridge, and subsequent separation by a hydrophilic end-capped Aquasil C18 columns with detection by tandem mass spectrometry using an electrospray ionization source in positive mode (ESI+). Recovery studies were carried out at three spiked levels (0.05, 0.1, 0.5 mg kg(-1)). The overall average recoveries using this method in green teas and black teas at the three concentration levels ranged from 76.15% to 101.86% with relative standard deviations (RSDs) in the range of 2.71-12.93% (n=5) for all analytes. The limits of detections (LODs) were below 0.009 mg kg(-1), which were lower than the maximum residue limits (MRLs) of 0.5 mg kg(-1) in tea samples established by the European Union legislations in 2008, while the limits of quantification (LOQ) did not exceed 0.03 mg kg(-1). This study provides a theoretical basis for China to draw up MRLs for pyrethrins in teas.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bridged Bicyclo Compounds / analysis
  • Bridged Bicyclo Compounds / isolation & purification
  • Chromatography, High Pressure Liquid / methods*
  • Insecticides / analysis*
  • Insecticides / isolation & purification
  • Pyrethrins / analysis*
  • Pyrethrins / isolation & purification
  • Solid Phase Extraction
  • Tandem Mass Spectrometry / methods*
  • Tea / chemistry*

Substances

  • Bridged Bicyclo Compounds
  • Insecticides
  • Pyrethrins
  • Tea
  • cinerin A
  • cinerin B
  • pyrethrin I