Oxidation of titanium-decorated single-walled carbon nanotubes and subsequent reduction by lithium

J Am Chem Soc. 2010 Apr 28;132(16):5789-92. doi: 10.1021/ja910976k.

Abstract

The chemical surface structure of Ti-decorated single-walled carbon nanotubes (SWNTs) is studied. X-ray photoelectron spectra show that Ti adatoms on the SWNT surface oxidize even under ultra-high-vacuum conditions, presenting a serious obstacle for the use of Ti-decorated SWNTs for hydrogen storage. A subsequent deposition of Li can, however, reduce the degree of Ti oxidation, "liberating" Ti atoms for the interaction with hydrogen molecules in hydrogen storage applications.