Highly enantioselective Michael addition of cyclopentanone with chalcones via novel di-iminium mechanism

Chem Commun (Camb). 2010 Mar 14;46(10):1751-3. doi: 10.1039/b915852a. Epub 2010 Jan 12.

Abstract

The highly efficient asymmetric Michael addition reactions of cyclopentanone with chalcones were catalyzed by a simple and commercially available chiral 1,2-diaminocyclohexane-hexanedioic acid, and exhibited good yields (up to 92%) and excellent enantioselectivities (up to 99% ee). A new di-iminium mechanism for the reaction was proposed.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Catalysis
  • Chalcone / chemistry*
  • Cyclopentanes / chemistry*
  • Stereoisomerism
  • Substrate Specificity
  • Temperature

Substances

  • Cyclopentanes
  • cyclopentanone
  • Chalcone