Pharmaceutical preparation of oxygen-15 labelled molecular oxygen and carbon monoxide gasses in a hospital setting

J Clin Pharm Ther. 2010 Feb;35(1):63-9. doi: 10.1111/j.1365-2710.2009.01032.x.

Abstract

Background: Clinical positron emission tomography (PET) requires safe and effective PET radiopharmaceuticals. Tracers used for measuring oxygen consumption and blood volume are [(15)O]O(2) and [(15)O]CO, respectively. In general, these oxygen-15 labelled tracers are produced using a cyclotron that accelerates deuterons onto a target filled with (14)N(2) containing a trace of oxygen. In recent years, cyclotrons have been developed that only are capable of accelerating protons. The purpose of this study was to validate and assess such a cyclotron for production and administration of oxygen-15 labelled gasses in an hospital setting.

Methods: An RDS111 cyclotron (Siemens-CTI, Knoxville, USA) was validated for bolus production of [(15)O]O(2) and [(15)O]CO gasses. In addition, equipment was developed to administer these tracers to patients.

Results: Both [(15)O]O(2) and [(15)O]CO gasses could be produced in sufficient amounts, whilst meeting European Pharmacopeia requirements. Although produced oxygen-15 gasses contained a minor level of (11)C contamination, in clinical studies it was possible to correct for this contamination by delayed blood counting.

Conclusion: An 11 MeV proton cyclotron combined with an in-house developed gas delivery system allows for the production and administration of sufficient amounts of [(15)O]-gasses for routine clinical PET studies in an hospital setting.

Publication types

  • Validation Study

MeSH terms

  • Administration, Inhalation
  • Blood Gas Analysis
  • Carbon Monoxide* / blood
  • Carbon Monoxide* / chemistry
  • Carbon Radioisotopes / blood
  • Carbon Radioisotopes / chemistry
  • Cyclotrons*
  • Drug Contamination
  • Humans
  • Insufflation / instrumentation
  • Oxygen Radioisotopes* / blood
  • Oxygen Radioisotopes* / chemistry
  • Oxygen* / blood
  • Oxygen* / chemistry
  • Positron-Emission Tomography* / instrumentation
  • Quality Control
  • Radiopharmaceuticals* / blood
  • Radiopharmaceuticals* / chemistry

Substances

  • Carbon Radioisotopes
  • Oxygen Radioisotopes
  • Radiopharmaceuticals
  • Carbon Monoxide
  • Oxygen