Conformational changes in guanylate cyclase-activating protein 1 induced by Ca2+ and N-terminal fatty acid acylation

Structure. 2010 Jan 13;18(1):116-26. doi: 10.1016/j.str.2009.11.008.

Abstract

Neuronal Ca(2+) sensors (NCS) are high-affinity Ca(2+)-binding proteins critical for regulating a vast range of physiological processes. Guanylate cyclase-activating proteins (GCAPs) are members of the NCS family responsible for activating retinal guanylate cyclases (GCs) at low Ca(2+) concentrations, triggering synthesis of cGMP and recovery of photoreceptor cells to the dark-adapted state. Here we use amide hydrogen-deuterium exchange and radiolytic labeling, and molecular dynamics simulations to study conformational changes induced by Ca(2+) and modulated by the N-terminal myristoyl group. Our data on the conformational dynamics of GCAP1 in solution suggest that Ca(2+) stabilizes the protein but induces relatively small changes in the domain structure; however, loss of Ca(+2) mediates a significant global relaxation and movement of N- and C-terminal domains. This model and the previously described "calcium-myristoyl switch" proposed for recoverin indicate significant diversity in conformational changes among these highly homologous NCS proteins with distinct functions.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Acylation
  • Amino Acid Sequence
  • Calcium / chemistry*
  • Calcium / metabolism
  • Deuterium Exchange Measurement
  • Fatty Acids / chemistry*
  • Fatty Acids / metabolism*
  • Guanylate Cyclase-Activating Proteins / chemistry*
  • Guanylate Cyclase-Activating Proteins / metabolism
  • Models, Molecular
  • Molecular Dynamics Simulation
  • Molecular Sequence Data
  • Protein Binding
  • Protein Structure, Tertiary

Substances

  • Fatty Acids
  • Guanylate Cyclase-Activating Proteins
  • Calcium