[Determination of apparent oil-water partition coefficient of andrographolide and dehydroandrographolide and effect of pH on them]

Zhong Yao Cai. 2009 Oct;32(10):1610-2.
[Article in Chinese]

Abstract

Objective: To determine the apparent n-octanol-water/buffer partition coefficient of andrographolide and dehydroandrographolide.

Methods: The apparent n-octanol-water/buffer partition coefficients of andrographolide and dehydroandrographolide were measured by shaking flask method. The concentrations of andrographolide and dehydroandrographolide were analyzed by HPLC method.

Results: The Papp of andrographolide and dehydroandrographolide were 3.90 (log Papp = 0.59) and 19.75 (log Papp = 1. 30) in water at 37 degrees C, respectively.

Conclusions: The apparent n-octanol-buffer partition coefficients of andrographolide and dehydroandrographolide are influenced by pH, and the higher pH may decrease the apparent n-octanol-buffer partition coefficients of them. Andrographolide has the highest partition coefficient in pH6, and dehydroandrogapholide in pH5.

Publication types

  • English Abstract
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Andrographis / chemistry*
  • Buffers
  • Chromatography, High Pressure Liquid / methods
  • Hydrogen-Ion Concentration
  • Lactones / chemistry*
  • Molecular Structure
  • Octanols
  • Oils / chemistry*
  • Plants, Medicinal / chemistry*
  • Solubility
  • Temperature
  • Water / chemistry*

Substances

  • Buffers
  • Lactones
  • Octanols
  • Oils
  • Water