Anti-inflammatory and vascularprotective properties of 8-prenylapigenin

Eur J Pharmacol. 2009 Oct 12;620(1-3):120-30. doi: 10.1016/j.ejphar.2009.08.015. Epub 2009 Aug 15.

Abstract

Flavonoids display several biological activities, but exhibit poor oral absorption and rapid metabolism. To improve their pharmacological profile four C8-prenyl flavonoids, structurally related to the anti-inflammatory lead apigenin, were synthesized, and the two least cytotoxic (IC(50)>30 microM) compounds [8-prenylnaringenin (8-PN) and 8-prenylapigenin (8-PA)] in RAW 264.7 murine macrophages were assayed against a panel of biological targets. The anti-inflammatory properties of these compounds were evaluated in an in vitro model of inflammation [cells exposed to 0.1 microg/ml lipopolysaccharide (LPS) for 24h]. Both 8-PN and 8-PA were equally effective and potent in inhibiting the LPS-induced gene expression [tumor necrosis factor (TNF)-alpha, inducible nitric oxide synthase (iNOS), cyclooxygenase (COX)-2] (RT-PCR) and release (ELISA) of pro-inflammatory mediators [TNF-alpha, NO, prostaglandin (PG)E(2)], through mechanisms involving the inhibition of nuclear factor-kappaB (NF-kappaB) activation (EMSA) and reactive oxygen species accumulation [2',7'-dichlorodihydrofluorescein diacetate (DCFH-DA) determination]. One-digit nM concentrations of 8-PN or 8-PA induced a significant increase in the basal production of the atheroprotective prostacyclin (PGI(2)) by human umbilical vein endothelial cells (HUVEC), with maximal effects at 10 nM. Both NS-398, a specific COX-2 inhibitor, and ICI 182 780, a non-selective estrogen receptor antagonist, abolished the activity of these compounds, suggesting a COX- and estrogen receptor-dependent mechanism of activity. 8-PA, a weaker estrogenic compound than 8-PN, resulted only 2-fold less potent than 8-PN in potentiating PGI(2) production by HUVEC, qualifying this C8-prenyl flavonoid as a lead for the rational design of new anti-inflammatory and vascularprotective compounds.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anti-Inflammatory Agents / chemistry
  • Anti-Inflammatory Agents / pharmacology*
  • Anti-Inflammatory Agents / toxicity
  • Antioxidants / pharmacology
  • Blood Vessels / drug effects*
  • Blood Vessels / metabolism
  • Cell Line
  • Cyclooxygenase 1 / metabolism
  • Cyclooxygenase 2 / metabolism
  • Dinoprostone / biosynthesis
  • Endothelial Cells / drug effects
  • Endothelial Cells / metabolism
  • Epoprostenol / biosynthesis
  • Flavanones / chemistry
  • Flavanones / pharmacology
  • Flavanones / toxicity
  • Flavones / chemistry
  • Flavones / pharmacology*
  • Flavones / toxicity
  • Gene Expression Regulation / drug effects
  • Humans
  • Mice
  • NF-kappa B / metabolism
  • Nitric Oxide / biosynthesis
  • Nitric Oxide Synthase Type II / metabolism
  • Prenylation
  • Tumor Necrosis Factor-alpha / metabolism

Substances

  • 8-prenylapigenin
  • 8-prenylnaringenin
  • Anti-Inflammatory Agents
  • Antioxidants
  • Flavanones
  • Flavones
  • NF-kappa B
  • Tumor Necrosis Factor-alpha
  • Nitric Oxide
  • Epoprostenol
  • Nitric Oxide Synthase Type II
  • Cyclooxygenase 1
  • Cyclooxygenase 2
  • Dinoprostone