[Studies on extraction of Ligusticum chuanxiong in Hongye Xintong soft capsule by super critical fluid extraction]

Zhongguo Zhong Yao Za Zhi. 2009 Jan;34(2):161-4.
[Article in Chinese]

Abstract

Objective: To study the rationality of extraction prosess for the Ligusticum chuanxiong in Hongye Xintong Soft Capsule by super critical fluid extraction(SFE).

Method: Conditions for the extraction were optimized by orthogonal experimental design as guided by the extraction rate and content of ligustilid in the extract; Combined with the experiment of rats ligated the left coronary artery, the two compounds containing different extracts (steam distillation and SFE) were compared to determine the extraction prosess.

Result: The best extraction conditions were established as following: pressure 30 MPa, temperature 50 degrees C, extracting time 4 h, separate pressure 10 MPa. separate temperature 40 degrees C. Compared with steam distillation, the compound containing SFE extract showed stronger protective effects on rats ligated the left coronary artery.

Conclusion: Super critical fluid can extract active ingredients in Ligusticum chuanxiong effectively.

MeSH terms

  • Animals
  • Capsules
  • Chromatography, Supercritical Fluid / methods*
  • Coronary Vessels / drug effects
  • Drugs, Chinese Herbal / chemistry*
  • Drugs, Chinese Herbal / isolation & purification
  • Drugs, Chinese Herbal / pharmacology
  • Female
  • Ligusticum
  • Male
  • Pressure
  • Rats
  • Temperature
  • Time Factors
  • Water / chemistry

Substances

  • Capsules
  • Drugs, Chinese Herbal
  • hongye xintong
  • Water
  • chuangxiong extract