Tretinoin-loaded nanocapsules: Preparation, physicochemical characterization, and photostability study

Int J Pharm. 2008 Mar 20;352(1-2):1-4. doi: 10.1016/j.ijpharm.2007.12.035. Epub 2008 Jan 3.

Abstract

The aim of this study was to prepare and characterize tretinoin-loaded nanocapsules as well as to evaluate the influence of this nanoencapsulation on tretinoin photostability. Tretinoin-loaded nanocapsules (0.5 mg ml(-1)) were prepared by interfacial deposition of preformed polymer (poly-epsilon-caprolactone) using two different oily phases: capric/caprylic triglycerides and sunflower seed oil. Tretinoin-loaded nanocapsules presented drug content close to the theoretical value, encapsulation efficiencies higher than 99.9%, nanometric mean size with a polydispersity index below 0.25, and pH values between 5.0 and 7.0. Regarding photodegradation studies, tretinoin methanolic solution showed a half-life time around 40 min according to a first order equation, whereas tretinoin nanocapsule suspensions showed a half-life between 85 and 100 min (twofold higher than in methanolic solution) according to a zero order equation. Tretinoin-loaded nanocapsules improved tretinoin photostability, independently on the type of oily phase used in this study, and represent a potential system to be incorporated in topical or systemic dosage forms containing tretinoin.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Caprylates / chemistry
  • Chemistry, Pharmaceutical
  • Decanoic Acids / chemistry
  • Dermatologic Agents / chemistry
  • Dermatologic Agents / radiation effects*
  • Drug Compounding
  • Drug Stability
  • Feasibility Studies
  • Half-Life
  • Kinetics
  • Nanocapsules*
  • Particle Size
  • Photolysis*
  • Plant Oils / chemistry
  • Polyesters / chemistry
  • Solubility
  • Sunflower Oil
  • Technology, Pharmaceutical / methods
  • Tretinoin / chemistry
  • Tretinoin / radiation effects*
  • Triglycerides / chemistry
  • Ultraviolet Rays*

Substances

  • Caprylates
  • Decanoic Acids
  • Dermatologic Agents
  • Nanocapsules
  • Plant Oils
  • Polyesters
  • Sunflower Oil
  • Triglycerides
  • polycaprolactone
  • Tretinoin