Integration of various stacking processes in carrier ampholyte-based capillary electrophoresis

J Chromatogr A. 2008 Feb 29;1182(2):226-32. doi: 10.1016/j.chroma.2007.12.079. Epub 2008 Jan 6.

Abstract

Field-enhanced sample stacking, field-enhanced sample injection as well as electrokinetic supercharging have been successfully integrated in carrier ampholyte-based capillary electrophoresis. Through the analysis of different test sample mixtures, it has been shown that the carrier ampholyte-based background electrolytes, in spite of their very low conductivity, allow efficient online preconcentration of analytes by field-amplified techniques. Sensitivity enhancement factors of the same magnitude as those usually encountered with classical conductive background electrolytes have been obtained in such carrier ampholyte-based buffers. Depending on the online preconcentration method that has been integrated, sensitivity enhancement factors between 50 and several thousands have been reached.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Ampholyte Mixtures
  • Animals
  • Buffers
  • Cytochromes c / analysis*
  • Electrolytes
  • Electrophoresis, Capillary / methods*
  • Heart
  • Horses
  • Isoelectric Focusing / methods*
  • Peptides / analysis*
  • Sensitivity and Specificity

Substances

  • Ampholyte Mixtures
  • Buffers
  • Electrolytes
  • Peptides
  • Cytochromes c