A one-dimensional nickel(II) coordination polymer containing 2,6-dipicolinate and dipyrido[3,2-a:2',3'-c]phenazine

Acta Crystallogr C. 2007 Dec;63(Pt 12):m573-5. doi: 10.1107/S0108270107053851. Epub 2007 Nov 24.

Abstract

A new coordination polymer, catena-poly[[(dipyrido[3,2-a:2',3'-c]phenazine-kappa(2)N,N')nickel(II)]-mu-2,6-dipicolinato-kappa(4)O(2),N,O(6):O(2')], [Ni(C7H3NO4)(C18H10N4)]n, exhibits a one-dimensional structure in which 2,6-dipicolinate acts as a bridging ligand interconnecting adjacent nickel(II) centers to form a chain structure. The asymmetric unit contains one Ni(II) center, one dipyrido[3,2-a:2',3'-c]phenazine ligand and one 2,6-dipicolinate ligand. Each Ni(II) center is six-coordinated and surrounded by three N atoms and three O atoms from one dipyrido[3,2-a:2',3'-c]phenazine ligand and two different 2,6-dipicolinate ligands, leading to a distorted octahedral geometry. Adjacent chains are linked by pi-pi stacking interactions and weak interactions to form a three-dimensional supramolecular network.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Crystallography, X-Ray
  • Iron Chelating Agents / chemistry
  • Molecular Structure
  • Nickel / chemistry*
  • Organometallic Compounds / chemical synthesis*
  • Organometallic Compounds / chemistry
  • Phenazines / chemistry*
  • Picolinic Acids / chemistry*
  • Polymers / chemical synthesis*
  • Polymers / chemistry

Substances

  • Iron Chelating Agents
  • Organometallic Compounds
  • Phenazines
  • Picolinic Acids
  • Polymers
  • catena-poly(((dipyrido(3,2-a-2',3'-c)phenazine-2N,N')nickel(II))-2,6-dipicolinato-4O2,N,O6-O2')
  • Nickel
  • picolinic acid