Investigation of the mechanisms of pulsed electric fields on inactivation of enzyme: lysozyme

J Agric Food Chem. 2007 Nov 28;55(24):9850-8. doi: 10.1021/jf072186s. Epub 2007 Oct 24.

Abstract

Lysozyme was selected as a model enzyme to investigate the effects of pulsed electric fields (PEF) on its activity and structure. The irreversible inactivation of lysozyme in sodium phosphate buffer (10 mM, pH 6.2) induced by PEF at 35 kV/cm followed a first-order model when the treatment time was longer than 300 micros. Unfolding of lysozyme structure was induced by PEF, accompanied by the cleavage of disulfide bonds and self-association aggregation when the applied PEF dosage was higher than a critical level. The inactivation of lysozyme by PEF was correlated to the loss of alpha-helix in secondary structure. The relative residual activity of PEF-treated lysozyme was in close agreement with the relative molar ellipticity at 208 nm. Both PEF- and heat-induced inactivations of lysozyme were correlated to the alteration of the secondary structure of lysozyme, but the effects of PEF and heat treatment on secondary structure were inconsistent.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Electric Stimulation*
  • Enzyme Inhibitors / chemistry
  • Enzyme Inhibitors / metabolism
  • Kinetics
  • Muramidase / antagonists & inhibitors
  • Muramidase / chemistry*
  • Muramidase / metabolism*
  • Protein Structure, Secondary

Substances

  • Enzyme Inhibitors
  • Muramidase