Polypeptide substrate specificity of PsLSMT. A set domain protein methyltransferase

J Biol Chem. 2007 Sep 21;282(38):27857-64. doi: 10.1074/jbc.M702069200. Epub 2007 Jul 17.

Abstract

Rubisco large subunit methyltransferase (PsLSMT) is a SET domain protein responsible for the trimethylation of Lys-14 in the large subunit of Rubisco. The polypeptide substrate specificity determinants for pea Rubisco large subunit methyltransferase were investigated using a fusion protein construct between the first 23 amino acids from the large subunit of Rubisco and human carbonic anhydrase II. A total of 40 conservative and non-conservative amino acid substitutions flanking the target Lys-14 methylation site (positions P(-3) to P(+3)) were engineered in the fusion protein. The catalytic efficiency (k(cat)/K(m)) of PsLSMT was determined using each of the substitutions and a polypeptide consensus recognition sequence deduced from the results. The consensus sequence, represented by X-(Gly/Ser)-(Phe/Tyr)-Lys-(Ala/Lys/Arg)-(Gly/Ser)-pi, where X is any residue, Lys is the methylation site, and pi is any aromatic or hydrophobic residue, was used to predict potential alternative substrates for PsLSMT. Four chloroplast-localized proteins were identified including gamma-tocopherol methyltransferase (gamma-TMT). In vitro methylation assays using PsLSMT and a bacterially expressed form of gamma-TMT from Perilla frutescens confirmed recognition and methylation of gamma-TMT by PsLSMT in vitro. RNA interference-mediated knockdown of the PsLSMT homologue (NtLSMT) in transgenic tobacco plants resulted in a 2-fold decrease of alpha-tocopherol, the product of gamma-TMT. The results demonstrate the efficacy of consensus sequence-driven identification of alternative substrates for PsLSMT as well as identification of functional attributes of protein methylation catalyzed by LSMT.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Catalysis
  • Histone-Lysine N-Methyltransferase / chemistry*
  • Kinetics
  • Lysine / chemistry
  • Methylation
  • Methyltransferases / chemistry
  • Nicotiana / genetics
  • Peptides / chemistry*
  • Perilla frutescens / enzymology*
  • Perilla frutescens / metabolism
  • Protein Methyltransferases / chemistry*
  • Protein Structure, Tertiary
  • RNA Interference
  • Ribulose-Bisphosphate Carboxylase / metabolism
  • Substrate Specificity
  • alpha-Tocopherol / metabolism

Substances

  • Peptides
  • Methyltransferases
  • Protein Methyltransferases
  • ribulose-1,5-bisphosphate carboxylase-oxygenase large subunit epsilonN-methyltransferase
  • Histone-Lysine N-Methyltransferase
  • gamma-tocopherol methyltransferase
  • Ribulose-Bisphosphate Carboxylase
  • alpha-Tocopherol
  • Lysine