[Studies on fingerprints of Bupleurum chinense from Hebei Province with HPLC-UV]

Zhong Yao Cai. 2006 Feb;29(2):119-23.
[Article in Chinese]

Abstract

Objective: To establish a HPLC fingerprint analysis method for identification of Bupleurum chinense of Hebei Province and compare the fingerprints of Radix Bupleuri collected from different habitats so as to establish a sensitive and specific method for controlling the quality of Radix Bupleuri.

Methods: The HPLC-UV fingerprints of Radix Bupleuri from different habitats were obtained from Waters 1525 instruments. The HPLC separation was performed on a C18 analytical column gradient eluted with a mixture consisting of acetonitrile and water at a flow rate of 1.0 ml/min with UV detector at 203 nm. The temperature of column was 30 degrees C.

Results: The mutual mode of HPLC-UV fingerprints was set up, and the similar degrees to the crude drugs of different habitats were compared.

Conclusion: It is simple and quick to differ Bupleurum chinense from different habitats with the method that can be used as a quality control item for Radix Bupleuri.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bupleurum / chemistry*
  • Bupleurum / classification
  • Chromatography, High Pressure Liquid / methods
  • Drug Stability
  • Oleanolic Acid / analogs & derivatives*
  • Oleanolic Acid / analysis
  • Oleanolic Acid / isolation & purification
  • Plant Roots / chemistry
  • Plants, Medicinal / chemistry*
  • Powders
  • Quality Control
  • Reproducibility of Results
  • Saponins / analysis*
  • Saponins / isolation & purification
  • Spectrophotometry, Ultraviolet / methods

Substances

  • Powders
  • Saponins
  • Oleanolic Acid
  • saikosaponin D