Quality control of anti-tuberculosis FDC formulations in the global market: part II-accelerated stability studies

Int J Tuberc Lung Dis. 2005 Nov;9(11):1266-72.

Abstract

Objective: To determine the quality and performance of rifampicin (RMP) containing fixed-dose combination (FDC) formulations of anti-tuberculosis drugs sourced from the international market with respect to physical, chemical and dissolution properties after storage at accelerated stability conditions (40 degrees C/75% relative humidity) and to identify appropriate storage specifications.

Methods: Formulations across different companies and combinations were subjected to 6-month accelerated stability testing in packaging conditions recommended by the manufacturer. Various pharmacopeial and nonpharmacopeial tests for tablets were performed for 3- and 6-month samples.

Results: All the formulations were found to be stable, where extent of dissolution was within +/- 10% of that of the initial value, and all formulations passed the pharmacopeial limits for assay and content uniformity of 90-110% and +/- 15% of average drug content, respectively.

Conclusions: Good quality RMP-containing FDCs that remain stable after 6-month accelerated stability testing are available in the marketplace.

MeSH terms

  • Antibiotics, Antitubercular / standards*
  • Drug Combinations
  • Drug Stability
  • Quality Control*
  • Rifampin / standards*
  • Time Factors

Substances

  • Antibiotics, Antitubercular
  • Drug Combinations
  • Rifampin