Purification, characterization, cDNA cloning, and expression of asialofetuin-binding C-type lectin from eggs of shishamo smelt (Osmerus [Spirinchus] lanceolatus)

Biochim Biophys Acta. 2005 Sep 15;1725(2):160-73. doi: 10.1016/j.bbagen.2005.07.009.

Abstract

A novel C-type lectin (OLABL) was isolated from the eggs of shishamo smelt [Osmerus (Spirinchus) lanceolatus] by affinity chromatography on asialofetuin-Sepharose. OLABL had a molecular mass of 29 kDa on SDS-PAGE under nonreducing conditions and two subunits with masses of 15 kDa (OLABL-H) and 14 kDa (OLABL-L) under reducing conditions. Thus, OLABL is a heterodimeric protein. cDNA sequence analysis revealed that the H- and L-subunits of OLABL were composed of 137 and 136 amino acid residues, respectively, and showed almost identical (95%) sequences, with slight differences in the N-terminal and C-terminal regions. Since each subunit contained only the characteristic motif of C-type lectin-like domain (CTLD), EPN-E-WND, OLABL is a member of group VII of the CTLD-containing protein family. Although OLABL had an EPN sequence that is known as a mannose-specific motif found in the collectin family, OLABL agglutinated rabbit erythrocytes without the addition of Ca(2+) ion, and this activity was inhibited by l-rhamnose and d-galactose derivatives, but not by d-mannose and d-glucose. These results indicate that OLABL has similar characteristics to AJL-2, a calcium-independent lactose specific lectin isolated from Japanese eel skin mucus. Recombinant OLABLs (rHisOLABLs), His-tagged homodimers of the H- and L-subunits, were refolded from inclusion bodies expressed by Escherichia coli. rHisOLABL-L was recovered as a soluble form, but rHisOLABL-H was hardly dissolved in a renaturing buffer. The specific activities of rHisOLABL-L, rHisOLABL-H, and native OLABL were 500, 36, and 20, respectively. These findings suggest that the combination of subunits may affect the solubility and activity of these dimeric form lectins.

MeSH terms

  • Agglutination / drug effects
  • Amino Acid Sequence
  • Animals
  • Asialoglycoproteins / metabolism*
  • Binding Sites
  • Calcium / metabolism*
  • Cells, Cultured
  • Cloning, Molecular
  • DNA, Complementary / genetics
  • Dose-Response Relationship, Drug
  • Egg Proteins / chemistry
  • Egg Proteins / pharmacology
  • Erythrocytes / drug effects*
  • Erythrocytes / immunology*
  • Fetuins
  • Humans
  • Lectins, C-Type / administration & dosage*
  • Lectins, C-Type / metabolism*
  • Molecular Sequence Data
  • Molecular Weight
  • Osmeriformes / metabolism*
  • Protein Binding
  • Rabbits
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / pharmacology
  • Sequence Homology, Amino Acid
  • alpha-Fetoproteins / metabolism*

Substances

  • Asialoglycoproteins
  • DNA, Complementary
  • Egg Proteins
  • Fetuins
  • Lectins, C-Type
  • Recombinant Proteins
  • alpha-Fetoproteins
  • asialofetuin
  • Calcium

Associated data

  • GENBANK/AB114832
  • GENBANK/AB114833