High-resolution 13C NMR studies of cellulose and cellulose oligomers in ionic liquid solutions

Chem Commun (Camb). 2005 Mar 28:(12):1557-9. doi: 10.1039/b417745b. Epub 2005 Jan 26.

Abstract

High-resolution 13C NMR studies of cellulose and cellulose oligomers dissolved in the ionic liquid (IL) 1-butyl-3-methylimidazolium chloride ([C4mim]Cl) show that the beta-(1-->4)-linked glucose oligomers are disordered in this medium and have a conformational behavior which parallels the one observed in water, and thus, reveal that the polymer is disordered in IL solution as well.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Carbon Isotopes
  • Cellulose / chemistry*
  • Imidazoles / chemistry
  • Ionic Liquids / chemistry*
  • Magnetic Resonance Spectroscopy
  • Solvents / chemistry

Substances

  • Carbon Isotopes
  • Imidazoles
  • Ionic Liquids
  • Solvents
  • 1-butyl-3-methylimidazolium chloride
  • Cellulose