Design, synthesis and photobiological properties of 3,4-cyclopentenepsoralens

Bioorg Med Chem. 2005 Feb 1;13(3):809-17. doi: 10.1016/j.bmc.2004.10.044.

Abstract

The QSAR directed synthesis of tetracyclic psoralen derivatives (3-5) characterised by the condensation of a cyclopentane ring at the level of the 3,4 double bond of the tricyclic psoralen moiety is reported. The new compounds present a methoxy (3), a hydroxy (4) or a dimethylaminopropoxy (5) side chain inserted in position 8 of the lead chromophore. The evaluation of photoantiproliferative activity on human tumour cell lines reveals for 5 an ability to inhibit cell growth significantly higher with respect to that of the reference drug, 8-MOP. Interestingly, the enhancement in antiproliferative activity is accompanied by the disappearance of skin phototoxicity. On the other hand, no significant photobiological activity was scored for 3 and 4. The ability to photoreact with DNA, evaluated by isolating the 4',5' monoadduct and by estimating the ability to form interstrand cross-links, appeared to be significant for 5, practically negligible for 3 and 4. Furthermore, a back-projection of the more active compound identifies structural features suitable for further synthetic modifications.

MeSH terms

  • Animals
  • Cell Division / drug effects
  • DNA / metabolism
  • Drug Design*
  • Furocoumarins / chemical synthesis*
  • Furocoumarins / chemistry
  • Furocoumarins / metabolism
  • Furocoumarins / pharmacology*
  • Guinea Pigs
  • HeLa Cells
  • Humans
  • Magnetic Resonance Spectroscopy
  • Photochemistry
  • Quantitative Structure-Activity Relationship
  • Skin / drug effects
  • Skin / radiation effects

Substances

  • Furocoumarins
  • DNA