Analysis of recombinant human saposin A expressed by Pichia pastoris

Biochem Biophys Res Commun. 2004 May 28;318(2):588-93. doi: 10.1016/j.bbrc.2004.04.069.

Abstract

Saposins (SAPs) are small glycoproteins required for activation of sphingolipid hydrolysis by lysosomal enzymes. Four SAPs, SAP-A, -B, -C, and -D, are proteolytically cleaved from a single gene product termed prosaposin. The mature coding sequence of human SAP-A tagged with 6-histidine was expressed in Pichia pastoris and the recombinant protein was purified from the culture supernatant by simple purification steps with an immobilized metal ion affinity column, a Concanavalin A column, and reversed-phase HPLC. Secreted SAP-A contained both glycosylated and nonglycosylated forms. Both forms of SAP-A activated galactocerebroside and 4-methylumbelliferyl beta-d-glucoside hydrolysis by galactocerebrosidase and glucocerebrosidase. SAP-A expressed in P. pastoris should be useful for further structural and functional analysis of this protein.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Binding Sites
  • Cloning, Molecular
  • Electrophoresis, Polyacrylamide Gel
  • Galactosylceramidase / metabolism
  • Gene Expression
  • Genes / genetics
  • Glycoproteins / genetics
  • Glycoproteins / isolation & purification
  • Glycoproteins / metabolism*
  • Glycosylation
  • Humans
  • Pichia / genetics
  • Pichia / metabolism*
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Recombinant Proteins / metabolism
  • Saposins

Substances

  • Glycoproteins
  • Recombinant Proteins
  • Saposins
  • Galactosylceramidase