Nitric oxide-induced formation of the S-2 state in the oxygen-evolving complex of photosystem II from Synechococcus elongatus

Biochemistry. 2003 Feb 4;42(4):1016-23. doi: 10.1021/bi026327p.

Abstract

In spinach photosystem II (PSII) membranes, the tetranuclear manganese cluster of the oxygen-evolving complex (OEC) can be reduced by incubation with nitric oxide at -30 degrees C to a state which is characterized by an Mn(2)(II, III) EPR multiline signal [Sarrou, J., Ioannidis, N., Deligiannakis, Y., and Petrouleas, V. (1998) Biochemistry 37, 3581-3587]. This state was recently assigned to the S(-)(2) state of the OEC [Schansker, G., Goussias, C., Petrouleas, V., and Rutherford, A. W. (2002) Biochemistry 41, 3057-3064]. On the basis of EPR spectroscopy and flash-induced oxygen evolution patterns, we show that a similar reduction process takes place in PSII samples of the thermophilic cyanobacterium Synechococcus elongatus at both -30 and 0 degrees C. An EPR multiline signal, very similar but not identical to that of the S(-)(2) state in spinach, was obtained with monomeric and dimeric PSII core complexes from S. elongatus only after incubation at -30 degrees C. The assignment of this EPR multiline signal to the S(-)(2) state is corroborated by measurements of flash-induced oxygen evolution patterns and detailed fits using extended Kok models. The small reproducible shifts of several low-field peak positions of the S(-)(2) EPR multiline signal in S. elongatus compared to spinach suggest that slight differences in the coordination geometry and/or the ligands of the manganese cluster exist between thermophilic cyanobacteria and higher plants.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cations / chemistry
  • Cyanobacteria / chemistry*
  • Cyanobacteria / metabolism*
  • Electron Spin Resonance Spectroscopy
  • Manganese / chemistry
  • Models, Chemical
  • Nitric Oxide / chemistry*
  • Oxidation-Reduction
  • Oxygen / chemistry
  • Oxygen / metabolism*
  • Photolysis
  • Photosynthetic Reaction Center Complex Proteins / chemistry
  • Photosynthetic Reaction Center Complex Proteins / metabolism*
  • Photosystem II Protein Complex
  • Spectrum Analysis, Raman
  • Spinacia oleracea
  • Thylakoids / chemistry
  • Thylakoids / metabolism

Substances

  • Cations
  • Photosynthetic Reaction Center Complex Proteins
  • Photosystem II Protein Complex
  • Nitric Oxide
  • Manganese
  • Oxygen