Artificial ribonucleases: efficient and specific in vitro cleavage of human c-raf-1 RNA

Bioconjug Chem. 2002 Sep-Oct;13(5):945-51. doi: 10.1021/bc0200024.

Abstract

We report here the first successful sequence-specific cleavage of large RNA using artificial ribonucleases. A series of uniformly 2'-methoxyethoxy-modified oligonucleotides bearing a europium complex were investigated as artificial ribonucleases specific for the human c-raf-1 mRNA. The efficiency and specificity of these oligonucleotide-metal conjugates to bind and to cleave 571 and 2,977 nucleotides long c-raf-1 RNA transcripts in vitro in a sequence-specific manner is demonstrated. Quantitative analysis reveals a cleavage efficiency of 60-70% within 4 h at 37 degrees C. Precise mapping of cleavage sites using primer extension analysis shows that cleavage generally occurs at two or three major sites adjacent to the 3'-end of the RNA target region. Cleavage is preferentially observed after purine nucleotides. This study demonstrates the potency of artificial ribonucleases targeting large, biologically relevant RNAs.

MeSH terms

  • Europium / chemistry
  • Humans
  • Hydrolysis / drug effects
  • Molecular Mimicry*
  • Oligonucleotides / chemical synthesis
  • Oligonucleotides / pharmacology
  • Proto-Oncogene Proteins c-raf / genetics*
  • RNA / metabolism*
  • Ribonucleases / chemical synthesis*
  • Ribonucleases / pharmacology
  • Substrate Specificity

Substances

  • Oligonucleotides
  • Europium
  • RNA
  • Proto-Oncogene Proteins c-raf
  • Ribonucleases