Structure of a polysaccharide from a Rhizobium species containing 2-deoxy-beta-D-arabino-hexuronic acid

Carbohydr Res. 2001 May 18;332(2):167-73. doi: 10.1016/s0008-6215(01)00080-5.

Abstract

The structure of the extracellular polysaccharide (EPS) produced by the Rhizobium sp. B strain isolated from atypical nodules on alfalfa has been determined using a combination of chemical and physical techniques (methylation analysis, high pH-anion exchange chromatography (HPAEC), mass spectrometry and 1-D and 2-D NMR spectroscopy). As opposed to the EPS from other strains of Rhizobium, the EPS from the sp. B strain contains D-Glc together with L-Rha and 2-deoxy-D-arabino-hexuronic acid. It is a polymer of a repeating unit having the following structure: --> 4)-beta-D-Glcp-(1 --> 4)-alpha-L-Rhap -(1 --> 3)-beta-D-Glcp-(1 --> 4)-2-deoxy-beta-D-GlcpA-(1 -->. The polysaccharide also contains 0.6 O-acetyl groups per sugar which have not been located.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acetylation
  • Carbohydrate Conformation
  • Carbohydrate Sequence
  • Chromatography, Ion Exchange
  • Gas Chromatography-Mass Spectrometry
  • Glucose / analysis
  • Medicago sativa / microbiology
  • Molecular Sequence Data
  • Nuclear Magnetic Resonance, Biomolecular
  • Polysaccharides, Bacterial / chemistry*
  • Polysaccharides, Bacterial / isolation & purification*
  • Rhamnose / analysis
  • Rhizobium / chemistry*
  • Rhizobium / isolation & purification

Substances

  • Polysaccharides, Bacterial
  • Glucose
  • Rhamnose