Charge engineering of a protein domain to allow efficient ion-exchange recovery

Protein Eng. 2000 Oct;13(10):703-9. doi: 10.1093/protein/13.10.703.

Abstract

We have created protein domains with extreme surface charge. These mutated domains allow for ion-exchange chromatography under conditions favourable for selective and efficient capture, using Escherichia coli as a host organism. The staphylococcal protein A-derived domain Z (Zwt) was used as a scaffold when constructing two mutants, Zbasic1 and Zbasic2, with high positive surface charge. Far-ultraviolet circular dichroism measurements showed that they have a secondary structure content comparable to the parental molecule Zwt. Although melting temperatures (Tm) of the engineered domains were lower than that of the wild-type Z domain, both mutants could be produced successfully as intracellular full-length products in E. coli and purified to homogeneity by ion-exchange chromatography. Further studies performed on Zbasic1 and Zbasic2 showed that they were able to bind to a cation exchanger even at pH values in the 9 to 11 range. A gene fusion between Zbasic2 and the acidic human serum albumin binding domain (ABD), derived from streptococcal protein G, was also constructed. The gene product Zbasic2-ABD could be purified using cation-exchange chromatography from a whole cell lysate to more than 90% purity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins / chemistry
  • Chromatography, Ion Exchange
  • Circular Dichroism
  • Escherichia coli / chemistry
  • Humans
  • Hydrogen-Ion Concentration
  • Mutagenesis, Site-Directed
  • Protein Denaturation
  • Protein Engineering
  • Protein Structure, Secondary
  • Protein Structure, Tertiary
  • Recombinant Fusion Proteins / chemistry*
  • Recombinant Fusion Proteins / genetics
  • Recombinant Fusion Proteins / isolation & purification*
  • Serum Albumin / chemistry
  • Staphylococcal Protein A / chemistry
  • Static Electricity
  • Thermodynamics

Substances

  • Bacterial Proteins
  • IgG Fc-binding protein, Streptococcus
  • Recombinant Fusion Proteins
  • Serum Albumin
  • Staphylococcal Protein A