Structure of a two-domain chitotriosidase from Serratia marcescens at 1.9-A resolution

Proc Natl Acad Sci U S A. 2000 May 23;97(11):5842-7. doi: 10.1073/pnas.97.11.5842.

Abstract

In this paper, we describe the structure of chitinase B from Serratia marcescens, which consists of a catalytic domain with a TIM-barrel fold and a 49-residue C-terminal chitin-binding domain. This chitinase is the first structure of a bacterial exochitinase, and it represents one of only a few examples of a glycosyl hydrolase structure having interacting catalytic and substrate-binding domains. The chitin-binding domain has exposed aromatic residues that contribute to a 55-A long continuous aromatic stretch extending into the active site. Binding of chitin oligomers is blocked beyond the -3 subsite, which explains why the enzyme has chitotriosidase activity and degrades the chitin chain from the nonreducing end. Comparison of the chitinase B structure with that of chitinase A explains why these enzymes act synergistically in the degradation of chitin.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acetylglucosamine / metabolism
  • Amino Acid Sequence
  • Bacterial Proteins / chemistry*
  • Binding Sites
  • Catalytic Domain
  • Chitin / metabolism
  • Chitinases / chemistry
  • Crystallography, X-Ray*
  • Hexosaminidases / chemistry*
  • Hydrogen Bonding
  • Models, Molecular
  • Molecular Sequence Data
  • Muramidase / chemistry
  • Plant Proteins / chemistry
  • Protein Conformation
  • Protein Structure, Tertiary
  • Sequence Alignment
  • Sequence Homology, Amino Acid
  • Serratia marcescens / enzymology*
  • Structure-Activity Relationship

Substances

  • Bacterial Proteins
  • Plant Proteins
  • Chitin
  • Hexosaminidases
  • chitotriosidase
  • Chitinases
  • PLC-B protein, Phytolacca americana
  • hevamine
  • Muramidase
  • Acetylglucosamine

Associated data

  • PDB/1E15